HPLC测定慢性盆腔炎丸中阿魏酸的含量
夏方亮
【期刊名称】《食品与药品》 【年(卷),期】2015(000)003
【摘要】Objective To establish an HPLC method for the determination of ferulic acid in Chronic Pelvic Inflammation Pills.Methods The C18 column was used with the mixture of acetonitrile-0.085 % phosphoric acid (14:86) as the mobile phase, and the detection wavelength was 316 nm.Results The standard curve of ferulic acid was linear in the range of 0.02049-0.2049μg (r=1.000,n=7), and the average recovery was 100.10 % (n=6). The limit of detection was 0.3073 ng and the limit of quantification was 1.0243 ng.Conclusion The method can be reliable, accurate and specific.%目的：建立高效液相色谱法测定慢性盆腔炎丸中阿魏酸的含量测定方法。方法用 C18柱为固定相，以乙腈-0.085%磷酸溶液（14：86）为流动相，检测波长为316 nm。结果阿魏酸进样量在0.02049～0.2049μg范围内呈良好的线性关系，r=1.000（n=7），其平均回收率（n=6）为100.10%。方法的检测限0.3073 ng，定量限1.0243 ng。结论此法可靠、准确、专属性强。 【总页数】3页(201-203) 【关键词】慢性盆腔炎丸;阿魏酸 【作者】夏方亮
【作者单位】滨州市食品药品检验检测中心，山东滨州 256618
HPLC测定慢性盆腔炎丸中阿魏酸的含量
