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第二部分 实验方案设计
实验目的：
1. 用P123合成介孔氧化硅模板SBA-15
2. 用介孔氧化硅为“硬模板”来合成有序介孔炭
所需化学试剂：
P123（聚环氧乙烯醚－聚环氧丙稀醚－聚环氧乙烯醚，摩尔比为20：70：20），正硅酸乙酯（TEOS，Aldrich）,蒸馏水，HCL（35 wt%）,乙醇，氢氟酸，蔗糖，硫酸
所需实验仪器：
烧杯，夹层烧杯，烘干箱，电磁搅拌器，电子天平，恒温水浴震荡器，比表面积和孔隙度测定仪，扫描电子显微镜，X－射线衍射仪
实验步骤：
2.4.1 氧化硅模板SBA-15的合成
(1)将32g P123（聚环氧乙烯醚－聚环氧丙稀醚－聚环氧乙烯醚，摩尔比为20：70：20）三嵌段聚合物表面活性剂（平均分子量为5800，分子式EO20PO70EO20，Aldrich）溶于1000g蒸馏水和200g HCL（35 wt%）中，在40℃下搅拌4个小时，以确保表面活性剂在水相体系中均匀分散。
(2)往溶液中加入68.8g正硅酸乙酯（TEOS，Aldrich），于40℃下搅拌15分钟，并在
40℃静置24小时。
(3)继续在40℃下陈化24小时。
(4)所得沉淀经过滤、并用乙醇洗涤。洗涤后的样品在550℃下焙烧2小时除去模板剂，所得样品标记为SBA-15-40。
(5)保持其它合成条件不变，仅改变陈化温度，分别在70℃和100℃下陈化24小时，所得到的样品分别标记为SBA-15-70和SBA-15-100。
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