常见溶剂的化学位移

常见溶剂的化学位移

常见溶剂的1H在不同氘代溶剂中的化学位移值

氘 代 溶 剂 CDCl3 (CD3)2CO (CD3)2SO C6D6 CD3CN CD3OD D2O 7.26 1.56 7.26 2.17 2.62 7.36 2.10 2.05 2.84 8.02 2.09 2.52 7.36 2.05 3.31 3.12 8.58 7.35 7.76 1.97 4.05 1.20 5.63 0.88 1.28 1.12 3.57 2.50 3.33 8.32 2.09 2.54 7.37 2.07 3.16 4.01 8.58 7.39 7.79 1.99 4.03 1.17 5.76 0.86 1.25 1.06 3.44 7.16 0.40 6.15 1.55 1.68 7.15 1.55 3.07 8.53 6.66 6.98 1.65 3.89 0.92 4.27 0.89 1.24 0.96 3.34 1.94 2.13 7.58 2.08 2.50 7.37 1.96 3.28 2.16 8.57 7.33 7.73 1.97 4.06 1.20 5.44 0.89 1.28 1.12 3.54 3.31 4.87 7.90 2.15 2.65 7.33 2.03 3.34 8.53 7.44 7.85 2.01 4.09 1.24 5.49 0.90 1.29 1.19 3.60 4.79 4.79 2.22 2.71 2.06 3.34 8.52 7.45 7.87 2.07 4.14 1.24 C5D5N 7.20 7.57 8.72 4.96 mult. 残余溶剂峰 水峰 CHCl3 (CH3)2CO (CH3)2SO C6H6 CH3CN CH3OH brs s s s s s 8.72 7.20 7.57 CH3,s 3.49 OH,s 1.09 8.62 CH(3),m 7.29 CH(4),m 7.68 CH(2),m C5H5N CH3,s CH3COOC2H5 CH2,q CH3,t 2.05 4.12 1.26 5.30 CH2Cl2 n-hexane C2H5OH s CH3,t CH3,t 1.17 3.65 0.88 CH2,m 1.26 1.25 CH2,q 3.72

常见溶剂的化学位移

常见溶剂的13C在不同氘代溶剂中的化学位移值

氘 代 溶 剂 CDCl3 (CD3)2CO (CD3)2SO 77.16 77.36 207.07 30.92 40.76 128.37 116.43 1.89 50.41 149.90 123.75 135.96 206.26 29.84 79.19 205.87 30.60 41.23 129.15 117.60 1.12 49.77 150.67 124.57 136.56 20.83 170.96 60.56 14.50 54.95 14.34 23.28 32.30 39.52 79.16 206.31 30.56 40.45 128.30 117.91 1.03 48.59 149.58 123.84 136.05 20.68 170.31 59.74 14.40 54.84 13.88 22.05 30.95 C6D6 128.06 77.79 204.43 30.14 40.03 128.62 116.02 0.20 49.97 150.27 123.58 135.28 20.56 170.44 60.21 14.19 53.46 14.32 23.04 31.96 CD3CN CD3OD 1.32 118.26 79.17 207.43 30.91 41.31 129.32 118.26 1.79 49.90 150.76 127.76 136.89 21.16 171.68 60.98 14.54 55.32 14.43 23.40 32.36 49.00 79.44 209.67 30.67 40.45 129.34 118.06 0.85 49.86 150.07 125.53 138.35 20.88 172.89 61.50 14.49 54.78 14.45 23.68 32.73 D2O - C5D5N 123.44 135.43 149.84 溶剂峰 CHCl3 (CH3)2CO (CH3)2SO C6H6 CH3CN CH3OH C5H5N 215.94 30.89 39.39 119.68 1.47 49.50 149.18 125.12 138.27 21.15 175.26 62.32 13.92 21.04 171.36 CH3COOC2H5 60.49 14.19 CH2Cl2 n-hexane

53.52 14.14 22.70 31.64