附 录 A （规范性附录） 实验室内重复性要求
?
实验室内重复性要求见表D.1。
表A.1 实验室内重复性要求
被测组分含量（mg/kg） ≤0.001 ＞0.001≤0.01 ＞0.01≤1 ＞0.1≤1 ＞1 精密度（%） 36 32 22 18 14 ? ? ? ? ? ? ? ? ? ? ?
B 附 录 B （规范性附录） 实验室间再现性要求
?
实验室间再现性要求见表E.1。
表B.1 实验室间再现性要求
被测组分含量（mg/kg） ≤0.001 ＞0.001≤0.01 ＞0.01≤1 ＞0.1≤1 ＞1 精密度（%） 54 46 34 25 19 ? C 附 录 C （资料性附录）
样品添加浓度及回收率的实验数据
? 果如下：
211种农药六种基质不同添加水平的回收率结
表C.1 211种农药六种基质不同添加水平的回收率
低水平添加（0.01 mg/kg） 猪肉 69.8% 85.7% 牛肉 83.5% 67.3% 羊肉 86.5% 84.0% 53.7% 76.5% 66.3% 肝脏 86.6% 75.3% 64.4% 76.2% 86.0% 牛奶 70.4% 73.3% 60.8% 鸡蛋 84.6% 75.4% 48.8% 猪肉 中水平添加（0.02 mg/kg） 牛肉 羊肉 70.3% 71.3% 48.5% 72.4% 67.1% 肝脏 81.3% 91.5% 83.0% 90.5% 牛奶 鸡蛋 猪肉 高水平添加（0.05 mg/k牛肉 羊肉 64.1% 70.1% 42.9% 62.0% 64.5% 肝脏 83.2% 73.3% 65.1% 74.9% 70.9% 77.2% 82.0% 79.2% 75.8% 93.5% 68.4% 70.5% 67.2% 92.4% 68.8% 74.2% 42.5% 67.9% 75.0% 73.1% 69.8% 85.5% 62.2% 113.5% 64.3% 75.7% 81.0% 84.7% 88.2% 92.7% 45.7% 81.7% 106.1% 81.4% 82.9% 71.8% 88.8% 84.7% 94.2% 77.1% 94.6% 90.4% 100.7% 67.7% 78.2% 82.4% 69.7% 101.1% 78.8% 80.3% 95.9% 75.7% 85.2% 113.5% 84.7% 84.5% 65.6% 108.9% 80.2% 62.2% 115.1% 65.0% 75.0% 61.8% 92.5% 63.6% 81.0% 87.3% 68.8% 83.7% 73.7% 71.6% 77.5% 97.0% 67.7% 76.8% 64.5% 79.0% 85.2% 83.0% 92.5% 84.0% 65.0% 95.9% 96.1% 78.8% 84.5% 80.2% 80.8% 72.0% 71.6% 86.2% 92.9% 90.4% 78.2% 77.3% 78.5% 69.0% 72.2% 76.0% 106.8% 113.7% 77.5% 113.6% 79.3% 103.4% 84.5% 96.8% 71.1% 109.0% ? ?
表F.1 211种农药六种基质不同添加水平的回收率（续）
低水平添加（0.01 mg/kg） 猪肉 87.5% 86.7% 牛肉 63.7% 76.5% 羊肉 87.7% 66.5% 肝脏 73.9% 73.4% 牛奶 76.7% 71.2% 鸡蛋 78.8% 84.0% 猪肉 80.8% 79.3% 中水平添加（0.02 mg/kg） 牛肉 62.3% 77.3% 羊肉 71.2% 79.1% 肝脏 99.7% 92.0% 牛奶 82.6% 95.0% 鸡蛋 61.7% 86.6% 猪肉 73.9% 73.6% 高水平添加（0.05 mg/k牛肉 61.2% 68.7% 羊肉 61.6% 72.1% 肝脏 68.3% 73.7% 117.0% 62.3% 112.5% 72.7% 84.5% 80.2% 90.9% 60.3% 79.0% 91.8% 95.0% 62.2% 83.2% 61.6% 62.0% 67.4% 103.8% 77.2% 74.2% 76.8% 68.7% 85.2% 73.6% 78.5% 63.8% 87.6% 91.1% 76.9% 77.7% 74.2% 64.3% 69.1% 105.3% 93.2% 74.7% 94.7% 67.7% 84.4% 82.3% 85.0% 68.3% 72.4% 95.7% 80.4% 78.7% 73.8% 64.3% 79.1% 103.5% 81.5% 74.2% 88.3% 78.2% 92.6% 80.0% 75.5% 70.3% 78.1% 94.8% 78.6% 67.7% 72.9% 65.1% 77.3% 104.0% 70.7% 83.0% 75.7% 87.5% 85.6% 95.0% 62.1% 68.5% 84.5% 100.9% 68.8% 85.7% 61.3% 63.8% 67.7% 低水平添加（0.01 mg/kg） 猪肉 88.3% 84.2% 86.0% 75.5% 牛肉 86.2% 80.8% 68.8% 93.3% 羊肉 74.5% 65.0% 77.0% 76.3% 肝脏 80.6% 71.9% 95.4% 88.4% 牛奶 73.2% 61.2% 79.7% 64.7% 鸡蛋 78.4% 64.1% 75.4% 67.1% 猪肉 79.0% 79.3% 75.3% 77.1% 中水平添加（0.02 mg/kg） 牛肉 82.6% 81.6% 81.6% 90.2% 羊肉 63.3% 62.0% 95.8% 63.9% 肝脏 79.4% 88.4% 106.5% 100.2% 牛奶 76.7% 75.3% 68.6% 58.8% 鸡蛋 76.9% 66.2% 75.4% 93.6% 猪肉 79.7% 75.6% 68.2% 76.1% 高水平添加（0.05 mg/k牛肉 78.7% 76.0% 68.5% 75.2% 羊肉 62.1% 62.5% 63.9% 61.3% 肝脏 67.8% 68.0% 80.6% 67.2%
表F.1 211种农药六种基质不同添加水平的回收率（续）
低水平添加（0.01 mg/kg） 猪肉 81.8% 86.0% 83.8% 73.8% 86.8% 72.5% 61.2% 95.5% 89.0% 85.0% 92.3% 96.3% 93.0% 86.2% 85.3% 91.0% 85.5% 84.8% 87.5% 牛肉 81.3% 71.2% 78.5% 75.0% 68.0% 77.3% 73.8% 64.3% 72.7% 71.5% 85.0% 羊肉 62.7% 68.3% 肝脏 76.9% 68.8% 牛奶 77.8% 69.2% 69.7% 74.3% 73.8% 86.8% 84.8% 64.3% 72.2% 65.0% 64.2% 69.7% 64.2% 65.8% 72.7% 80.7% 68.0% 69.8% 72.7% 鸡蛋 65.0% 66.4% 75.8% 80.1% 73.3% 96.7% 65.1% 74.5% 68.2% 67.4% 60.2% 50.5% 57.6% 72.3% 84.9% 85.8% 84.2% 77.1% 76.4% 猪肉 74.0% 77.4% 75.1% 76.0% 85.9% 67.7% 69.9% 86.8% 74.7% 66.8% 79.1% 中水平添加（0.02 mg/kg） 牛肉 78.3% 76.6% 84.0% 86.5% 92.5% 91.7% 76.3% 66.4% 82.8% 70.8% 85.4% 羊肉 63.9% 63.5% 肝脏 96.8% 85.6% 牛奶 鸡蛋 猪肉 高水平添加（0.05 mg/牛肉 69.5% 73.0% 79.6% 72.6% 77.9% 76.1% 68.7% 64.3% 69.0% 65.0% 73.9% 羊肉 肝脏 磷 81.8% 64.3% 67.2% 82.3% 63.6% 72.4% 61.3% 76.1% 磷 63.4% 74.2% 66.3% 107.4% 66.8% 93.8% 77.7% 84.5% 87.7% 66.0% 66.7% 53.2% 78.5% 71.8% 87.4% 74.1% 74.6% 75.7% 70.9% 71.4% 65.9% 64.8% 65.4% 75.5% 78.0% 76.0% 74.4% 71.6% 63.9% 104.6% 88.2% 72.2% 76.4% 69.7% 94.8% 88.5% 90.8% 95.1% 67.2% 75.1% 86.1% 62.7% 74.2% 66.0% 83.3% 61.2% 76.9% 85.3% 81.4% 64.6% 104.7% 80.4% 91.5% 67.9% 70.4% 77.4% 61.8% 62.0% 43.8% 73.7% 96.7% 83.4% 85.4% 81.8% 80.5% 91.3% 98.0% 77.2% 93.9% 85.1% 86.6% 90.7% 79.5% 68.5% 61.8% 74.9% 62.9% 80.5% 73.4% 64.2% 73.0% 74.8% 67.0% 72.4% 85.8% 54.0% 79.8% 61.5% 84.2% 双 67.2% 73.4% 70.3% 74.3% 61.9% 73.6% 64.6% 70.3% 44.1% 67.7% 105.8% 74.8% 74.8% 96.8% 76.8% 87.7% 94.5% 70.5% 73.8% 63.5% 84.8% 66.2% 82.3% 72.3% 88.8% 70.5% 80.5% 116.8% 67.2% 84.3% 83.5% 78.1% 77.9% 79.6% 79.5% 79.3% 78.2% 83.8% 78.9% 83.5% 89.0% 72.5% 75.8% 62.6% 71.8% 63.2% 67.1% 64.9% 79.8% 62.8% 81.3% 46.9% 74.7% 103.7% 62.2% 67.9% 88.3% 52.3% 77.2% 82.7% 85.4% 71.1% 89.8% 77.6% 75.9% 90.8% 86.4% 76.8% 83.4% 74.3% 76.1% 80.8% 89.4% 81.6% 90.7% 67.1% 76.1% 70.2% 87.1% 72.8% 78.6% 77.5% 63.1% 71.0% 62.7% 70.2% 溴66.0% 67.6% 62.0% 62.8% 74.5% 77.5% 醇 67.5% 74.8% 69.8% 70.2% 64.5% 72.8% 表F.1 211种农药六种基质不同添加水平的回收率（续）
低水平添加（0.01 mg/kg） 猪肉 85.3% 牛肉 65.7% 羊肉 83.3% 72.5% 81.8% 肝脏 82.5% 62.1% 75.8% 牛奶 80.3% 77.0% 75.7% 鸡蛋 75.0% 72.5% 84.5% 猪肉 中水平添加（0.02 mg/kg） 牛肉 羊肉 70.7% 75.1% 73.9% 肝脏 87.7% 72.0% 91.5% 牛奶 93.1% 88.3% 88.4% 鸡蛋 69.2% 79.5% 78.3% 猪肉 74.5% 74.1% 65.2% 高水平添加（0.05 mg/牛肉 羊肉 肝脏 78.8% 71.8% 76.3% 73.6% 75.4% 69.4% 66.7% 68.5% 68.4% 109.2% 65.0% 95.5% 68.2% 71.2% 73.1% 68.9% 63.7% 63.9% 73.3% 低水平添加（0.01 mg/kg） 猪肉 75.5% 74.5% 牛肉 84.0% 64.5% 羊肉 75.7% 78.8% 84.5% 77.5% 78.5% 84.2% 84.3% 64.8% 84.5% 74.3% 84.8% 肝脏 62.1% 72.7% 87.4% 84.3% 63.9% 94.2% 84.5% 63.3% 82.9% 73.0% 77.4% 牛奶 66.8% 84.0% 83.8% 66.0% 74.8% 62.5% 67.8% 65.5% 78.5% 67.8% 69.3% 鸡蛋 86.3% 84.9% 94.9% 77.1% 89.0% 83.9% 76.3% 84.2% 猪肉 中水平添加（0.02 mg/kg） 牛肉 羊肉 65.9% 81.1% 71.8% 68.4% 70.7% 68.8% 63.9% 65.6% 78.1% 64.2% 67.6% 肝脏 87.4% 93.2% 95.2% 85.3% 77.7% 83.4% 87.7% 84.6% 92.6% 87.2% 91.1% 牛奶 84.7% 87.5% 89.5% 80.5% 93.8% 68.6% 75.8% 78.2% 87.6% 85.9% 86.8% 鸡蛋 87.6% 77.7% 90.5% 76.0% 85.6% 74.5% 69.6% 74.9% 94.6% 87.0% 81.4% 猪肉 63.4% 62.4% 75.3% 75.1% 66.1% 72.7% 72.6% 66.3% 65.6% 74.0% 63.4% 高水平添加（0.05 mg/牛肉 羊肉 肝脏 72.9% 83.4% 72.1% 67.2% 76.4% 88.9% 72.1% 84.0% 76.8% 83.2% 74.9% 77.8% 70.7% 82.6% 76.3% 80.4% 78.7% 62.6% 65.5% 62.7% 65.8% 73.0% 105.8% 91.0% 77.2% 76.0% 85.2% 76.3% 86.2% 79.7% 77.3% 77.2% 75.3% 83.8% 78.3% 70.0% 79.7% 78.3% 90.2% 76.2% 77.9% 71.4% 84.2% 79.1% 63.7% 79.4% 77.2% 66.5% 65.8% 75.5% 68.5% 76.8% 75.1% 62.7% 75.5% 77.8% 71.6% 69.3% 103.6% 77.3% 94.3% 85.0% 86.4% 77.2% 81.8% 78.8% 75.8% 78.2% 61.9% 74.6% 75.2% 62.5% 68.5% 71.1% 61.9% 72.3% 滴95.8% 77.5% 65.7% 74.9% 69.3% 64.1% 77.0% 84.0% 66.8% 86.1% 83.2% 61.2% 74.0% 79.0% 64.1% 71.1%
表F.1 211种农药六种基质不同添加水平的回收率（续）
低水平添加（0.01 mg/kg） 猪肉 95.5% 牛肉 72.0% 羊肉 67.3% 肝脏 74.5% 牛奶 63.2% 鸡蛋 66.4% 猪肉 76.3% 中水平添加（0.02 mg/kg） 牛肉 82.3% 羊肉 62.3% 肝脏 84.9% 牛奶 77.9% 鸡蛋 63.4% 猪肉 73.0% 高水平添加（0.05 mg/k牛肉 74.1% 羊肉 62.7% 肝脏 72.4% 78.5% 72.3% 62.7% 68.6% 64.7% 64.3% 78.6% 75.1% 63.3% 84.9% 80.9% 62.8% 74.1% 69.1% 62.9% 65.4% 78.7% 68.7% 86.5% 65.2% 55.3% 56.6% 76.0% 73.3% 64.8% 81.3% 71.3% 50.0% 71.6% 67.3% 62.7% 64.3% 96.0% 78.3% 62.0% 72.4% 69.2% 45.6% 77.3% 75.1% 66.4% 89.1% 81.3% 65.3% 80.0% 72.0% 63.6% 72.5% 96.3% 67.2% 77.5% 68.7% 86.5% 95.0% 75.3% 76.5% 87.2% 63.5% 88.3% 66.0% 66.3% 65.2% 81.3% 80.5% 52.2% 76.3% 64.2% 79.8% 85.2% 77.0% 68.7% 68.0% 83.1% 74.7% 75.9% 99.4% 73.3% 75.2% 82.6% 68.0% 84.2% 72.8% 65.7% 63.7% 69.7% 68.2% 76.3% 75.8% 42.5% 77.0% 74.9% 73.8% 65.3% 67.7% 94.1% 84.4% 76.4% 71.9% 65.6% 71.2% 79.6% 84.1% 74.4% 73.3% 79.8% 61.5% 78.2% 83.5% 72.8% 72.2% 83.9% 83.4% 51.8% 74.6% 72.2% 63.3% 73.6% 66.1% 68.6% 65.6% 86.4% 89.5% 95.8% 81.3% 91.2% 88.9% 94.7% 84.7% 95.6% 80.0% 68.5% 69.8% 85.4% 82.2% 79.9% 93.7% 53.3% 64.6% 72.2% 69.2% 67.5% 63.1% 98.2% 80.3% 76.0% 63.9% 65.0% 67.6% 73.2% 75.3% 63.6% 64.7% 75.3% 61.3% 76.1% 76.4% 68.3% 66.1% 74.0% 75.5% 47.4% 62.6% 65.4% 66.6% 65.9% 62.9% 63.9% 61.5% 71.9% 74.6% 74.9% 77.8% 68.4% 70.0% 77.4% 68.7%
动物源性食品中211种农药及相关化学品样品添加浓度及回收率的实验数据
